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organic chemistry distillation lab: The Organic Chem Lab Survival Manual James W. Zubrick, 2020-02-05 Teaches students the basic techniques and equipment of the organic chemistry lab — the updated new edition of the popular hands-on guide. The Organic Chem Lab Survival Manual helps students understand the basic techniques, essential safety protocols, and the standard instrumentation necessary for success in the laboratory. Author James W. Zubrick has been assisting students navigate organic chemistry labs for more than three decades, explaining how to set up the laboratory, make accurate measurements, and perform safe and meaningful experiments. This practical guide covers every essential area of lab knowledge, from keeping detailed notes and interpreting handbooks to using equipment for chromatography and infrared spectroscopy. Now in its eleventh edition, this guide has been thoroughly updated to cover current laboratory practices, instruments, and techniques. Focusing primarily on macroscale equipment and experiments, chapters cover microscale jointware, drying agents, recrystallization, distillation, nuclear magnetic resonance, and much more. This popular textbook: Familiarizes students with common lab instruments Provides guidance on basic lab skills and procedures Includes easy-to-follow diagrams and illustrations of lab experiments Features practical exercises and activities at the end of each chapter Provides real-world examples of lab notes and instrument manuals The Organic Chem Lab Survival Manual: A Student’s Guide to Techniques, 11th Edition is an essential resource for students new to the laboratory environment, as well as those more experienced seeking to refresh their knowledge. |
organic chemistry distillation lab: Techniques in Organic Chemistry Jerry R. Mohrig, Christina Noring Hammond, Paul F. Schatz, 2010-01-06 Compatible with standard taper miniscale, 14/10 standard taper microscale, Williamson microscale. Supports guided inquiry--Cover. |
organic chemistry distillation lab: The Organic Chem Lab Survival Manual James W. Zubrick, 2003-07-31 Publisher Description |
organic chemistry distillation lab: Laboratory Technique in Organic Chemistry Kenneth B. Wiberg, 1960 |
organic chemistry distillation lab: Organic Chemistry with Vernier Elaine Y. Nam, Melissa P. Hill, Jack Randall, 2020-09 |
organic chemistry distillation lab: Purification of Laboratory Chemicals W.L.F. Armarego, 2003-03-07 Now in its fifth edition, the book has been updated to include more detailed descriptions of new or more commonly used techniques since the last edition as well as remove those that are no longer used, procedures which have been developed recently, ionization constants (pKa values) and also more detail about the trivial names of compounds.In addition to having two general chapters on purification procedures, this book provides details of the physical properties and purification procedures, taken from literature, of a very extensive number of organic, inorganic and biochemical compounds which are commercially available. This is the only complete source that covers the purification of laboratory chemicals that are commercially available in this manner and format.* Complete update of this valuable, well-known reference* Provides purification procedures of commercially available chemicals and biochemicals* Includes an extremely useful compilation of ionisation constants |
organic chemistry distillation lab: Advanced Practical Organic Chemistry, Second Edition John Leonard, Barry Lygo, Garry Procter, 1994-06-02 The first edition of this book achieved considerable success due to its ease of use and practical approach, and to the clear writing style of the authors. The preparation of organic compounds is still central to many disciplines, from the most applied to the highly academic and, more tan ever is not limited to chemists. With an emphasis on the most up-to-date techniques commonly used in organic syntheses, this book draws on the extensive experience of the authors and their association with some of the world's mleading laboratories of synthetic organic chemistry. In this new edition, all the figures have been re-drawn to bring them up to the highest possible standard, and the text has been revised to bring it up to date. Written primarily for postgraduate, advanced undergraduate and industrial organic chemists, particularly those involved in pharmaceutical, agrochemical and other areas of fine chemical research, the book is also a source of reference for biochemists, biologists, genetic engineers, material scientists and polymer researchers. |
organic chemistry distillation lab: Comprehensive Organic Chemistry Experiments for the Laboratory Classroom Carlos A. M. Afonso, Nuno R. Candeias, Dulce Pereira Simão, Alexandre F. Trindade, Jaime A. S. Coelho, Bin Tan, Robert Franzén, 2016-12-16 This expansive and practical textbook contains organic chemistry experiments for teaching in the laboratory at the undergraduate level covering a range of functional group transformations and key organic reactions.The editorial team have collected contributions from around the world and standardized them for publication. Each experiment will explore a modern chemistry scenario, such as: sustainable chemistry; application in the pharmaceutical industry; catalysis and material sciences, to name a few. All the experiments will be complemented with a set of questions to challenge the students and a section for the instructors, concerning the results obtained and advice on getting the best outcome from the experiment. A section covering practical aspects with tips and advice for the instructors, together with the results obtained in the laboratory by students, has been compiled for each experiment. Targeted at professors and lecturers in chemistry, this useful text will provide up to date experiments putting the science into context for the students. |
organic chemistry distillation lab: Organic Laboratory Techniques Ralph J. Fessenden, Joan S. Fessenden, Patty Feist, 2001 This highly effective and practical manual is designed to be used as a supplementary text for the organic chemistry laboratory course - and with virtually any main text - in which experiments are supplied by the instructor or in which the students work independently. Each technique contains a brief theoretical discussion. Steps used in each technique, along with common problems that might arise. These respected and renowned authors include supplemental or related procedures, suggested experiments, and suggested readings for many of the techniques. Additionally, each chapter ends with a set of study problems that primarily stress the practical aspects of each technique, and microscale techniques are included throughout the text, as appropriate. Additional exercises, reference material, and quizzes are available online. |
organic chemistry distillation lab: Laboratory Manual for Organic Chemistry Kenneth F. Cerny, Christopher E. Katz, 2017-07-20 |
organic chemistry distillation lab: Operational Organic Chemistry John W. Lehman, 1988 |
organic chemistry distillation lab: Making the Connections Anne Padias, Joshua Osbourn, 2023-01-30 |
organic chemistry distillation lab: Practical Organic Synthesis Reinhart Keese, Martin P. Brändle, Trevor P. Toube, 2006-06-16 Success in an experimental science such as chemistry depends on good laboratory practice, a knowledge of basic techniques, and the intelligent and careful handling of chemicals. Practical Organic Synthesis is a concise, useful guide to good laboratory practice in the organic chemistry lab with hints and tips on successful organic synthesis. Topics covered include: safety in the laboratory environmentally responsible handling of chemicals and solvents crystallisation distillation chromatographic methods extraction and work-up structure determination by spectroscopic methods searching the chemical literature laboratory notebooks writing a report hints on the synthesis of organic compounds disposal and destruction of dangerous materials drying and purifying solvents Practical Organic Synthesis is based on a successful course in basic organic chemistry laboratory practice which has run for several years at the ETH, Zurich and the University of Berne, and its course book Grundoperationen, now in its sixth edition. Condensing over 30 years of the authors’ organic laboratory teaching experience into one easy-to-read volume, Practical Organic Synthesis is an essential guide for those new to the organic chemistry laboratory, and a handy benchtop guide for practising organic chemists. |
organic chemistry distillation lab: Whisky Science Gregory H. Miller, |
organic chemistry distillation lab: Organic Experiments Louis Frederick Fieser, Kenneth L. Williamson, 1987 |
organic chemistry distillation lab: The Dare Harley Laroux, 2023-10-31 Jessica Martin is not a nice girl. As Prom Queen and Captain of the cheer squad, she'd ruled her school mercilessly, looking down her nose at everyone she deemed unworthy. The most unworthy of them all? The freak, Manson Reed: her favorite victim. But a lot changes after high school. A freak like him never should have ended up at the same Halloween party as her. He never should have been able to beat her at a game of Drink or Dare. He never should have been able to humiliate her in front of everyone. Losing the game means taking the dare: a dare to serve Manson for the entire night as his slave. It's a dare that Jessica's pride - and curiosity - won't allow her to refuse. What ensues is a dark game of pleasure and pain, fear and desire. Is it only a game? Only revenge? Only a dare? Or is it something more? The Dare is an 18+ erotic romance novella and a prequel to the Losers Duet. Reader discretion is strongly advised. This book contains graphic sexual scenes, intense scenes of BDSM, and strong language. A full content note can be found in the front matter of the book. |
organic chemistry distillation lab: Experiments in Organic Chemistry Louis Frederick Fieser, 1935 |
organic chemistry distillation lab: Microscale and Miniscale Organic Chemistry Laboratory Experiments Allen Schoffstall, Barbara Gaddis, Melvin Druelinger, 2003-07-08 This book offers a comprehensive introductory treatment of the organic laboratory techniques for handling glassware and equipment, safety in the laboratory, micro- and miniscale experimental procedures, theory of reactions and techniques, relevant background information, applications and spectroscopy. |
organic chemistry distillation lab: Techniques and Experiments for Organic Chemistry Addison Ault, 1976 |
organic chemistry distillation lab: Organic Chemistry I Lab Manual David Modarelli, Modarelli Et Al, Yi Pang, Zhexi Li, 2020-08-17 |
organic chemistry distillation lab: Technique of Organic Chemistry: Distillation Arnold Weissberger, 1945 |
organic chemistry distillation lab: Laboratory manual of organic chemistry Harry Linn Fisher, 1920 |
organic chemistry distillation lab: Green Organic Chemistry Kenneth M. Doxsee, James E. Hutchison, 2004 This lab text describes the tools and strategies of green chemistry, and the lab experiments that allow investigation of organic chemistry concepts and techniques in a greener laboratory setting. Students acquire the tools to assess the health and environmental impacts of chemical processes and the strategies to improve develop new processes that are less harmful to human health and the environment. The curriculum introduces a number of state-of-the-art experiments and reduces reliance on expensive environmental controls, such as fume hoods.--Provided by publisher. |
organic chemistry distillation lab: Experimental Organic Chemistry Daniel R. Palleros, 2000-02-04 This cutting-edge lab manual takes a multiscale approach, presenting both micro, semi-micro, and macroscale techniques. The manual is easy to navigate with all relevant techniques found as they are needed. Cutting-edge subjects such as HPLC, bioorganic chemistry, multistep synthesis, and more are presented in a clear and engaging fashion. |
organic chemistry distillation lab: Chemical Demonstrations Bassam Z. Shakhashiri, 1985 Describes and gives instructions for lecture demonstrations covering acids and bases and liquids, solutions, and colloids |
organic chemistry distillation lab: Experiments in Organic Chemistry Richard K. Hill, Hill Richard K.., John Barbaro, 2000 |
organic chemistry distillation lab: Systematic Lab Experiments in Organic Chemistry Arun Sethi, 2006 Basically The Book Has Been Written As A Textbook With An Intention To Serve The Students At The Graduate And Postgraduate Level. The Subject Matter Is Based On The New Model Curriculum Recommended By The University Grants Commission For All Indian Universities. The Book Provides An Exhaustive List Of Organic Compounds, Methods Of Its Identification, Its Derivatives Every Information Incorporated In Consolidated Form. Exercises Included In The Book Not Only Describe Different Methods/Techniques Of Preparation But Also Explain The Theoretical Background Of These Reactions. It Also Describes Different Methods Of Isolation Of Some Important Class Of Compounds. This Book Promotes Self Reliance Since It Is In Itself Complete Requiring No Reference To Other Texts. |
organic chemistry distillation lab: Techniques and Experiments For Organic Chemistry Addison Ault, 1998-08-12 Embraced by the inside covers' periodic table of elements and table of solutions of acids, the new edition of this introductory text continues to describe laboratory operations in its first part, and experiments in the second. Revisions by Ault (Cornell U.) include detailed instructions for the disposal of waste, and experiments with more interesting compounds (e.g. seven reactions of vanillin, and isolating ibuprofin from ibuprofin tablets). Conscious of costs, microscale experiments are included but not to the point where minuscule amounts of material will preclude the aesthetic pleasure of watching crystals form or distillates collect. Annotation copyrighted by Book News, Inc., Portland, OR |
organic chemistry distillation lab: Experiments and Exercises in Basic Chemistry Steven Murov, Brian Stedjee, 2003-03-12 Taking an exploratory approach to chemistry, this hands-on lab manual for preparatory chemistry encourages critical thinking and allows students to make discoveries as they experiment. A set of exercises provides students with additional opportunities to test their understanding of key concepts in introductory and prep chemistry courses. Written in a clear, easy-to-read style. Numerous experiments to choose from cover all topics typically covered in prep chemistry courses. Chemical Capsules demonstrate the relevance and importance of chemistry. |
organic chemistry distillation lab: Illustrated Guide to Home Chemistry Experiments Robert Bruce Thompson, 2012-02-17 For students, DIY hobbyists, and science buffs, who can no longer get real chemistry sets, this one-of-a-kind guide explains how to set up and use a home chemistry lab, with step-by-step instructions for conducting experiments in basic chemistry -- not just to make pretty colors and stinky smells, but to learn how to do real lab work: Purify alcohol by distillation Produce hydrogen and oxygen gas by electrolysis Smelt metallic copper from copper ore you make yourself Analyze the makeup of seawater, bone, and other common substances Synthesize oil of wintergreen from aspirin and rayon fiber from paper Perform forensics tests for fingerprints, blood, drugs, and poisons and much more From the 1930s through the 1970s, chemistry sets were among the most popular Christmas gifts, selling in the millions. But two decades ago, real chemistry sets began to disappear as manufacturers and retailers became concerned about liability. ,em>The Illustrated Guide to Home Chemistry Experiments steps up to the plate with lessons on how to equip your home chemistry lab, master laboratory skills, and work safely in your lab. The bulk of this book consists of 17 hands-on chapters that include multiple laboratory sessions on the following topics: Separating Mixtures Solubility and Solutions Colligative Properties of Solutions Introduction to Chemical Reactions & Stoichiometry Reduction-Oxidation (Redox) Reactions Acid-Base Chemistry Chemical Kinetics Chemical Equilibrium and Le Chatelier's Principle Gas Chemistry Thermochemistry and Calorimetry Electrochemistry Photochemistry Colloids and Suspensions Qualitative Analysis Quantitative Analysis Synthesis of Useful Compounds Forensic Chemistry With plenty of full-color illustrations and photos, Illustrated Guide to Home Chemistry Experiments offers introductory level sessions suitable for a middle school or first-year high school chemistry laboratory course, and more advanced sessions suitable for students who intend to take the College Board Advanced Placement (AP) Chemistry exam. A student who completes all of the laboratories in this book will have done the equivalent of two full years of high school chemistry lab work or a first-year college general chemistry laboratory course. This hands-on introduction to real chemistry -- using real equipment, real chemicals, and real quantitative experiments -- is ideal for the many thousands of young people and adults who want to experience the magic of chemistry. |
organic chemistry distillation lab: Introduction to Organic Laboratory Techniques Donald L. Pavia, Gary M. Lampman, George S. Kriz, Randall G. Engel, 2005 Featuring 66 experiments, detailing 29 techniques, and including several explicating essays, this lab manual covers basic lab techniques, molecular modeling, properties and reactions of organic compounds, the identification of organic substances, project-based experiments, and each step of the various techniques. The authors teach at Western Washington University and North Seattle Community College. Annotation ♭2004 Book News, Inc., Portland, OR (booknews.com). |
organic chemistry distillation lab: Experimental Organic Chemistry John C. Gilbert, Stephen F. Martin, 2002-01-01 |
organic chemistry distillation lab: Unitized Experiments in Organic Chemistry Ray Quincy Brewster, Calvin Anthony VanderWerf, William Edwin McEwen, 1977 |
organic chemistry distillation lab: A Microscale Approach to Organic Laboratory Techniques Donald L. Pavia, George S. Kriz, Gary M. Lampman, Randall G. Engel, 2016-12-05 Featuring new experiments unique to this lab textbook, as well as new and revised essays and updated techniques, this Sixth Edition provides the up-to-date coverage students need to succeed in their coursework and future careers. From biofuels, green chemistry, and nanotechnology, the book’s experiments, designed to utilize microscale glassware and equipment, demonstrate the relationship between organic chemistry and everyday life, with project-and biological or health science focused experiments. As they move through the book, students will experience traditional organic reactions and syntheses, the isolation of natural products, and molecular modeling. Important Notice: Media content referenced within the product description or the product text may not be available in the ebook version. |
organic chemistry distillation lab: Microscale Organic Laboratory Dana W. Mayo, Ronald M. Pike, Peter K. Trumper, 1994-05-06 This updated revision offers total coverage of organic laboratory experiments and techniques focusing on modern laboratory instrumentation, a strong emphasis on lab safety, additional concentration on sequential reaction sequences, excellent pre- and post-lab exercises, and multistep experiments which maximize the number of manipulations students perform per lab period. The microscale approach is low in cost, offers ease of doing experiments and uses minimal amounts of chemicals. A number of experiments include instructions for scaling up. |
organic chemistry distillation lab: The Golden Book of Chemistry Experiments Robert Brent, 2015-10-10 BANNED: The Golden Book of Chemistry Experiments was a children's chemistry book written in the 1960s by Robert Brent and illustrated by Harry Lazarus, showing how to set up your own home laboratory and conduct over 200 experiments. The book is controversial, as many of the experiments contained in the book are now considered too dangerous for the general public. There are apparently only 126 copies of this book in libraries worldwide. Despite this, its known as one of the best DIY chemistry books every published. The book was a source of inspiration to David Hahn, nicknamed the Radioactive Boy Scout by the media, who tried to collect a sample of every chemical element and also built a model nuclear reactor (nuclear reactions however are not covered in this book), which led to the involvement of the authorities. On the other hand, it has also been the inspiration for many children who went on to get advanced degrees and productive chemical careers in industry or academia. |
organic chemistry distillation lab: Practical Organic Chemistry Frederick George Mann, Bernard Charles Saunders, 1975 A Clear And Reliable Guide To Students Of Practical Organic Chemistry At The Undergraduate And Postgraduate Levels. This Edition S Special Emphasis Is On Semi Micro Methods And Modern Techniques And Reactions. |
organic chemistry distillation lab: Purification of Laboratory Chemicals W.L.F. Armarego, Christina Li Lin Chai, 2013 A best seller since 1966, Purification of Laboratory Chemicals keeps engineers, scientists, chemists, biochemists and students up to date with the purification of the chemical reagents with which they work, the processes for their purification, and guides readers on critical safety and hazards for the safe handling of chemicals and processes. The Seventh Edition is fully updated and provides expanded coverage of the latest commercially available chemical products and processing techniques, safety and hazards: over 200 pages of coverage of new commercially available chemicals since the previous edition. The only comprehensive chemical purification reference, a market leader since 1966, Amarego delivers essential information for research and industrial chemists, pharmacists and engineers: '... (it) will be the most commonly used reference book in any chemical or biochemical laboratory' (MDPI Journal) An essential lab practice and proceedures manual. Improves efficiency, results and safety by providing critical information for day-to-day lab and processing work. Improved, clear organization and new indexing delivers accurate, reliable information on processes and techniques of purification along with detailed physical properties The Sixth Edition has been reorganised and is fully indexed by CAS Registry Numbers; compounds are now grouped to make navigation easier; literature references for all substances and techniques have been added; ambiguous alternate names and cross references removed; new chemical products and processing techniques are covered; hazards and safety remain central to the book |
organic chemistry distillation lab: Techniques in Organic Chemistry Jerry R. Mohrig, Christina Noring Hammond, Paul F. Schatz, 2006 Is the most comprehensive and detailed presentation of lab techniques available for organic chemistry students - and the least expensive. It combines specific instructions for 3 different kinds kinds of laboratory glassware and offers extensive coverage of spectroscopic techniques and a strong emphasis on safety issues. |
organic chemistry distillation lab: Microscale Organic Laboratory Dana W. Mayo, Ronald M. Pike, David C. Forbes, 2010-01-12 This is a laboratory text for the mainstream organic chemistry course taught at both two and four year schools, featuring both microscale experiments and options for scaling up appropriate experiments for use in the macroscale lab. It provides complete coverage of organic laboratory experiments and techniques with a strong emphasis on modern laboratory instrumentation, a sharp focus on safety in the lab, excellent pre- and post-lab exercises, and multi-step experiments. Notable enhancements to this new edition include inquiry-driven experimentation, validation of the purification process, and the implementation of greener processes (including microwave use) to perform traditional experimentation. |
ORGANIC LABORATORY TECHNIQUES 10 - Faculty of Science
Distillation is a separation process that involves heating a liquid to its boiling point, transferring the vapour to a different portion of the apparatus, then condensing the vapour and collecting the …
Organic Chemistry 211 Laboratory Simple Distillation
Organic Chemistry 211 Laboratory Simple Distillation In this experiment simple distillation will be performed in order to separate ethyl acetate from butyl acetate. Assemble the apparatus as …
Distillation - Tishk International University
Distillation involves the conversion of a liquid to its vapor upon heating, then cooling the vapor by (Liebig Condenser) to condense and collecting it into the flask. Practical Organic Chemistry …
Organic Chemistry Lab 1: Simple Distillation
Distillation • An important organic process used to separate two or more than two liquids having different boiling points from a liquid mixture. • Distillation based on the boiling point of the liquid …
CHEM 344 Distillation of liquid mixtures - University of Wisconsin ...
The vaporization of a liquid and condensation of the resulting vapor is the basis of distillation. Organic liquids containing small amounts (<15%) of impurities or non-volatile substances are …
SOP: DISTILLATION - University of Cape Town
Distillation is the process of heating a liquid until it boils, then condensing and collecting the resultant hot vapours. In the modern organic chemistry laboratory, distillation is a powerful …
ORGANIC CHEMISTRY LABORATORY TECHNIQUES - Labflow
The goal of the project was twofold: a) to create a free electronic laboratory resource for students, b) to show greater step-by-step detail for organic chemistry lab techniques than is usually …
FRACTIONAL AND SIMPLE DISTILLATION OF …
Fractional distillation is used because it can complete several little distillations, or theoretical plates, in one distillation. The purity of each fraction isolated during the distillation is measured …
Microsoft Word - Lab 2 Distillation_handout FS2010.doc
In a normal chemistry lab, we use distillation for purification of starting materials, solvents, and products. In various experiments in organic chemistry lab, you will be performing both simple …
Justin Barry Professor Bill Dailey Chemistry 502 Experiment #2, …
In this experiment, we will separate 2 distillates using their differences in boiling points. The boiling points of individual liquids are affected by the impurities of the mixture. Each liquid will …
Simple Distillation - Flinn Sci
Distillation is used in organic chemistry labs and in the chemical process industry (e.g., petroleum refining) to purify compoundsand to separate the components in a mixture. It is also the oldest …
Fractional And Simple Distillation Lab Report
Organic Chemistry Lab 1: Simple Distillation Simple distillation. It is a process of separation & purification of liquid organic compounds by selective evaporation & condensation.
PHARMACEUTICAL ORGANIC CHEMISTRY II LAB MANUAL
Steam distillation finds application in the separation of such compounds from mixtures containing nonvolatile impurities, as well as in the isolation of steam-volatile organic compounds from …
ORGANIC CHEMISTRY LABORATORY EXPERIMENTS FOR …
Purification of compounds that are either synthesized in the lab or that have been isolated from sources in nature is a very important part of organic chemistry. A variety of methods may be …
E24 PURIFICATION OF ORGANIC COMPOUNDS Distillation, …
Distillation is the process of vaporising a sample, condensing the vapour, and collecting the condensate in another vessel. Each volatile component of the mixture can thus be distilled …
LABORATORY 4 Fractional Distillation - Stockton Wordpress
Organic Chemistry: Techniques and Transformations LABORATORY 4 Fractional Distillation Concept goals: Role of fractionating column and when such a column is necessary, refraction …
CH361/361H Week 6 Lecture Simple and Fractional Distillation
Distillation Set-Ups for This Week • Grignard: after work-up, distill off ether, then conduct dehydration/distillation of 2-ene
Writing an Organic Chemistry Lab Report - Miami University
The first time you do a technique, such as distillation, include in the procedure section a description of how to assemble the apparatus and how to conduct the distillation.
Distillation and Gas Chromatography - Winthrop University
Distillation is a technique often used to purify a liquid or to separate liquid components of a mixture. Essentially, it is the process of converting a liquid (called the distilland) to vapor by …
The Organic Chem Lab Survival Manual - Shroomery
sections on the theory of extraction and distillation, including azeotropes and azeotropic distillation, and, I believe, the first application of the Clausius-Clapyron equation as a bridge for …
ORGANIC LABORATORY TECHNIQUES 10 - Faculty of S…
Distillation is a separation process that involves heating a liquid to its …
Organic Chemistry 211 Laboratory Simple Distillation
Organic Chemistry 211 Laboratory Simple Distillation In this experiment …
Distillation - Tishk International University
Distillation involves the conversion of a liquid to its vapor upon heating, …
Organic Chemistry Lab 1: Simple Distillation
Distillation • An important organic process used to separate two or …
CHEM 344 Distillation of liquid mixtures - University of Wisco…
The vaporization of a liquid and condensation of the resulting vapor …